{"id":1996,"date":"2022-07-08T09:50:02","date_gmt":"2022-07-08T08:50:02","guid":{"rendered":"https:\/\/www.jeoljason.com\/2022\/07\/08\/%e7%b5%90%e5%90%88%e5%ae%9a%e6%95%b0%e3%82%92%e6%b8%ac%e3%82%8b%ef%bc%9apart1\/"},"modified":"2022-07-08T09:50:02","modified_gmt":"2022-07-08T08:50:02","slug":"%e7%b5%90%e5%90%88%e5%ae%9a%e6%95%b0%e3%82%92%e6%b8%ac%e3%82%8b%ef%bc%9apart1","status":"publish","type":"post","link":"https:\/\/www.jeoljason.com\/ja\/2022\/07\/08\/%e7%b5%90%e5%90%88%e5%ae%9a%e6%95%b0%e3%82%92%e6%b8%ac%e3%82%8b%ef%bc%9apart1\/","title":{"rendered":"\u7d50\u5408\u5b9a\u6570\u3092\u6e2c\u308b\uff1apart1"},"content":{"rendered":"<p>NMR\u5206\u5149\u6cd5\u306b\u304a\u3044\u3066\u3001<sup>1<\/sup>H\u3068<sup>13<\/sup>C\u306e\u3088\u3046\u306a\u6838\u9593\u306e\u7570\u7a2e\u6838\u30b9\u30d4\u30f3-\u30b9\u30d4\u30f3\u7d50\u5408\u306f\u8c4a\u5bcc\u306a\u5316\u5b66\u69cb\u9020\u60c5\u5831\u3092\u63d0\u4f9b\u3057\u307e\u3059\u3002\u3057\u304b\u3057\u306a\u304c\u3089\u3001\u6642\u306b\u306f\u60c5\u5831\u304c\u591a\u3059\u304e\u308b\u3053\u3068\u3084<sup>1<\/sup>H-<sup>1<\/sup>H\u30b9\u30ab\u30e9\u30fc\u30ab\u30c3\u30d7\u30ea\u30f3\u30b0\u306e\u3088\u3046\u306a\u7af6\u5408\u3059\u308b\u60c5\u5831\u306b\u60d1\u308f\u3055\u308c\u308b\u3053\u3068\u304c\u554f\u984c\u3068\u306a\u308a\u307e\u3059\u3002\u8907\u96d1\u306aNMR\u30b9\u30da\u30af\u30c8\u30eb\u3092\u5358\u7d14\u5316\u3057\u305f\u308a\u3001\u7d50\u5408\u5b9a\u6570\u306e\u6e2c\u5b9a\u3092\u5bb9\u6613\u306b\u3057\u305f\u308a\u3059\u308b\u305f\u3081\u3001\u3053\u308c\u307e\u3067\u9577\u5e74\u306b\u308f\u305f\u3063\u3066\u3001\u6570\u591a\u304f\u306e\u975e\u5e38\u306b\u30a8\u30ec\u30ac\u30f3\u30c8\u3067\u8208\u5473\u6df1\u3044NMR\u306e\u624b\u6cd5\u304c\u958b\u767a\u3055\u308c\u3066\u304d\u307e\u3057\u305f\u3002\u3053\u308c\u304b\u3089\u3044\u304f\u3064\u304b\u306e\u6295\u7a3f\u3092\u901a\u3057\u3066\u3001\u6700\u3082\u91cd\u8981\u3067\u6c4e\u7528\u7684\u306a\u65b9\u6cd5\u306b\u95a2\u3059\u308b\u7c21\u5358\u306a\u6982\u8981\u3092\u63d0\u793a\u3057\u3088\u3046\u3068\u601d\u3044\u307e\u3059\u3002\u6700\u521d\u306e\u6295\u7a3f\u3067\u306f\u3001\u6570\u3042\u308b\u5b9f\u9a13\u624b\u6cd5\u306e\u4e2d\u3067\u3082\u6700\u3082\u30b7\u30f3\u30d7\u30eb\u306a\u9078\u629e\u7684\u30c7\u30ab\u30c3\u30d7\u30ea\u30f3\u30b0\u3092\u9ad8\u5206\u89e3\u80fd<sup>13<\/sup>C\u30b9\u30da\u30af\u30c8\u30eb\u306b\u4f7f\u7528\u3057\u305f\u4f8b\u3092\u793a\u3057\u307e\u3059\u3002\u4ee5\u4e0b\u306b\u793a\u3059\u30c7\u30fc\u30bf\u306f<a href=\"https:\/\/www.jeol.co.jp\/en\/products\/detail\/ROYALPROBE_HFX.html\">ROYAL-HFX\u30d7\u30ed\u30fc\u30d6<\/a>\u3092\u5099\u3048\u305f3\u30c1\u30e3\u30f3\u30cd\u30eb\u306e\u00a0<a href=\"https:\/\/www.jeol.co.jp\/en\/products\/detail\/JNM-ECZL.html\">JEOL ECZ-500<\/a>\u5206\u5149\u8a08\u3067\u6e2c\u5b9a\u3057\u3001<a href=\"https:\/\/www.jeoljason.com\/ja\/\">JASON\u30bd\u30d5\u30c8\u30a6\u30a7\u30a2<\/a>\u306b\u3088\u3063\u3066\u89e3\u6790\u3092\u884c\u3063\u305f\u3082\u306e\u3067\u3059\u3002<\/p>\n<p>&nbsp;<\/p>\n<h3>\u4e8c\u91cd\u5171\u9cf4\u6cd5<\/h3>\n<p>\u4e8c\u91cd\u5171\u9cf4NMR\uff08\u30c7\u30ab\u30c3\u30d7\u30ea\u30f3\u30b0\uff09\u306e\u30a2\u30a4\u30c7\u30a2\u306fNMR\u304c\u51fa\u59cb\u3081\u305f\u9803\u306bWeston A. Anderson\u306e\u8ad6\u6587\u306e\u4e2d\u3067\u751f\u307e\u308c\u307e\u3057\u305f\u3002\u305d\u306eWes\uff08Weston\uff09\u306e\u4ed5\u4e8b\u3092\u542b\u307f\u30011950\u5e74\u4ee3\u521d\u982d\uff08\u5316\u5b66\u8005\u304cNMR\u3092\u898b\u3064\u3051\u305f\u9803\uff09\u306eNMR\u306b\u95a2\u3059\u308b\u975e\u5e38\u306b\u826f\u3044\u30ec\u30d3\u30e5\u30fc\u306bRay Freeman\u306e\u30d6\u30ed\u30b0\uff08<a href=\"http:\/\/ray-freeman.org\/nmr-history.html\">http:\/\/ray-freeman.org\/nmr-history.html<\/a>\uff09\u304c\u3042\u308a\u307e\u3059\u3002\u3053\u306e\u6587\u7ae0\u306f\u3001\u5553\u8499\u7684\u3067\u6b74\u53f2\u7684\u306b\u91cd\u8981\u306a\u3060\u3051\u3067\u306a\u304f\u3001\u8aad\u3093\u3067\u3044\u3066\u975e\u5e38\u306b\u697d\u3057\u3044\u3082\u306e\u3067\u3082\u3042\u308a\u307e\u3059\u3002<\/p>\n<p>&nbsp;<\/p>\n<h3>\u30d1\u30fc\u30d5\u30eb\u30aa\u30ed\u5206\u5b50\u306e\u4f8b<\/h3>\n<p>\u5358\u7d14\u306a\u30d5\u30c3\u7d20\u5316\u5408\u7269\u3092\u7528\u3044\u3066\u3001\u4e8c\u91cd\u5171\u9cf4\u6cd5\u3092\u4f7f\u3063\u305f\u7d50\u5408\u5b9a\u6570\u3092\u6e2c\u308b\u5fdc\u7528\u4f8b\u306b\u3064\u3044\u3066\u8aac\u660e\u3057\u307e\u3057\u3087\u3046\u3002\u3053\u3053\u3067\u7b54\u3048\u306a\u3051\u308c\u3070\u3044\u3051\u306a\u3044\u554f\u984c\u3068\u3044\u3046\u306e\u306f\u201cF2, F5, F6\u304b\u3089\u305d\u308c\u305e\u308c\u306e\u70ad\u7d20\u3078\u8907\u6570\u898b\u3089\u308c\u308b<sup>19<\/sup>F-<sup>13<\/sup>C\u7d50\u5408\u5b9a\u6570\u306e\u5024\u306f\u4f55\u306a\u306e\u304b\uff1f\u201d\u3068\u3044\u3046\u3053\u3068\u3067\u3059\u3002\u3053\u306e\u554f\u984c\u306e\u7b54\u3048\u3092\u5f97\u308b\u3053\u3068\u306f\u4fe1\u3058\u3089\u308c\u306a\u3044\u307b\u3069\u7c21\u5358\u3067\u3059\uff01\u307e\u305a\u3001F2, F5, F6\u3044\u305a\u308c\u304b\u306b\u9078\u629e\u7684<sup>19<\/sup>F\u30c7\u30ab\u30c3\u30d7\u30ea\u30f3\u30b0\u3092\u884c\u3063\u305f3\u3064\u306e<sup>13<\/sup>C\u30b9\u30da\u30af\u30c8\u30eb\u306e\u30c7\u30fc\u30bf\u30bb\u30c3\u30c8\u3092\u53d6\u5f97\u3057\u307e\u3059\u3002\u6b21\u306b\u3001\u30c7\u30ab\u30c3\u30d7\u30ea\u30f3\u30b0\u3092\u3057\u3066\u3044\u306a\u3044<sup>13<\/sup>C\u30b9\u30da\u30af\u30c8\u30eb\u3068\u6bd4\u8f03\u3057\u3001\u76ee\u7684\u306e\u7d50\u5408\u5b9a\u6570\u306e\u60c5\u5831\u3092\u5165\u529b\u3057\u305f\u8868\u3092\u4f5c\u6210\u3057\u307e\u3059\u3002<\/p>\n<p>&nbsp;<\/p>\n<p><img data-recalc-dims=\"1\" decoding=\"async\" class=\"alignnone wp-image-1416\" src=\"https:\/\/i0.wp.com\/www.jeoljason.com\/wp-content\/uploads\/2022\/03\/13C19F-spectra-perfluorinated-molecule-1.png?resize=901%2C468&#038;ssl=1\" alt=\"\" width=\"901\" height=\"468\" srcset=\"https:\/\/i0.wp.com\/www.jeoljason.com\/wp-content\/uploads\/2022\/03\/13C19F-spectra-perfluorinated-molecule-1.png?resize=200%2C104&amp;ssl=1 200w, https:\/\/i0.wp.com\/www.jeoljason.com\/wp-content\/uploads\/2022\/03\/13C19F-spectra-perfluorinated-molecule-1.png?resize=300%2C156&amp;ssl=1 300w, https:\/\/i0.wp.com\/www.jeoljason.com\/wp-content\/uploads\/2022\/03\/13C19F-spectra-perfluorinated-molecule-1.png?resize=400%2C208&amp;ssl=1 400w, https:\/\/i0.wp.com\/www.jeoljason.com\/wp-content\/uploads\/2022\/03\/13C19F-spectra-perfluorinated-molecule-1.png?resize=500%2C260&amp;ssl=1 500w, https:\/\/i0.wp.com\/www.jeoljason.com\/wp-content\/uploads\/2022\/03\/13C19F-spectra-perfluorinated-molecule-1.png?resize=600%2C311&amp;ssl=1 600w, https:\/\/i0.wp.com\/www.jeoljason.com\/wp-content\/uploads\/2022\/03\/13C19F-spectra-perfluorinated-molecule-1.png?resize=700%2C363&amp;ssl=1 700w, https:\/\/i0.wp.com\/www.jeoljason.com\/wp-content\/uploads\/2022\/03\/13C19F-spectra-perfluorinated-molecule-1.png?resize=768%2C399&amp;ssl=1 768w, https:\/\/i0.wp.com\/www.jeoljason.com\/wp-content\/uploads\/2022\/03\/13C19F-spectra-perfluorinated-molecule-1.png?resize=800%2C415&amp;ssl=1 800w, https:\/\/i0.wp.com\/www.jeoljason.com\/wp-content\/uploads\/2022\/03\/13C19F-spectra-perfluorinated-molecule-1.png?resize=1024%2C532&amp;ssl=1 1024w, https:\/\/i0.wp.com\/www.jeoljason.com\/wp-content\/uploads\/2022\/03\/13C19F-spectra-perfluorinated-molecule-1.png?resize=1200%2C623&amp;ssl=1 1200w, https:\/\/i0.wp.com\/www.jeoljason.com\/wp-content\/uploads\/2022\/03\/13C19F-spectra-perfluorinated-molecule-1.png?resize=1536%2C797&amp;ssl=1 1536w, https:\/\/i0.wp.com\/www.jeoljason.com\/wp-content\/uploads\/2022\/03\/13C19F-spectra-perfluorinated-molecule-1.png?w=1880&amp;ssl=1 1880w\" sizes=\"(max-width: 901px) 100vw, 901px\" \/><\/p>\n<p>(1) \u624b\u77ed\u306b\u3068\u3063\u305f 1D <sup>13<\/sup>C\u306f\u69d8\u3005\u306a\u9078\u629e\u7684\u30c7\u30ab\u30c3\u30d7\u30ea\u30f3\u30b0\u6761\u4ef6\u3067\u53d6\u5f97\u3057\u307e\u3057\u305f\u3002\u8d64\u3044\u77e2\u5370\u306f\u5404\u30b9\u30da\u30af\u30c8\u30eb\u306b\u304a\u3044\u3066\u76f4\u63a5\u7d50\u5408\u3057\u3066\u3044\u308b<sup>13<\/sup>C\u306e\u4f4d\u7f6e\u3092\u793a\u3057\u3066\u3044\u307e\u3059\u3002<\/p>\n<p>\u3053\u306e3\u3064\u306e\u9078\u629e\u7684<sup>19<\/sup>F\u30c7\u30ab\u30c3\u30d7\u30ea\u30f3\u30b0\u5b9f\u9a13\u3067\u3001\u3059\u3079\u3066\u306e<em>J<\/em><sub>FC<\/sub>\u3092\u5b8c\u5168\u306b\u6c7a\u3081\u308b\u3053\u3068\u304c\u3067\u304d\u307e\u3059\u3002<\/p>\n<p>\u6ce8\u76ee\u3059\u308b\u70ad\u7d20\u306e\u4fe1\u53f7\u3092\u4e2d\u5fc3\u306b\u30b9\u30da\u30af\u30c8\u30eb\u3092\u62e1\u5927\u3059\u308b\u3068\u3001\u5168\u3066\u306e\u30ab\u30c3\u30d7\u30ea\u30f3\u30b0\u304c\u660e\u78ba\u306b\u3001\u307e\u305f\u7c21\u5358\u306b\u62bd\u51fa\u3067\u304d\u307e\u3059\u3002\u4f8b\u3068\u3057\u3066\u30012\u3064\u306e\u62e1\u5927\u30b9\u30da\u30af\u30c8\u30eb\u3092\u793a\u3057\u307e\u3059\uff1b1\u3064\u306f\u30d5\u30c3\u7d20\u306b\u76f4\u63a5\u7d50\u5408\u3057\u305fC-5\u3001\u3082\u30461\u3064\u306f\u56db\u7d1a\u70ad\u7d20\u306eC-4\u3067\u3059\u3002<\/p>\n<p>&nbsp;<\/p>\n<p><img data-recalc-dims=\"1\" decoding=\"async\" class=\"alignnone wp-image-1418\" src=\"https:\/\/i0.wp.com\/www.jeoljason.com\/wp-content\/uploads\/2022\/03\/13C19F-spectra-perfluorinated-molecule-expansion-1.png?resize=898%2C476&#038;ssl=1\" alt=\"\" width=\"898\" height=\"476\" srcset=\"https:\/\/i0.wp.com\/www.jeoljason.com\/wp-content\/uploads\/2022\/03\/13C19F-spectra-perfluorinated-molecule-expansion-1.png?resize=200%2C106&amp;ssl=1 200w, https:\/\/i0.wp.com\/www.jeoljason.com\/wp-content\/uploads\/2022\/03\/13C19F-spectra-perfluorinated-molecule-expansion-1.png?resize=300%2C159&amp;ssl=1 300w, https:\/\/i0.wp.com\/www.jeoljason.com\/wp-content\/uploads\/2022\/03\/13C19F-spectra-perfluorinated-molecule-expansion-1.png?resize=400%2C211&amp;ssl=1 400w, https:\/\/i0.wp.com\/www.jeoljason.com\/wp-content\/uploads\/2022\/03\/13C19F-spectra-perfluorinated-molecule-expansion-1.png?resize=500%2C264&amp;ssl=1 500w, https:\/\/i0.wp.com\/www.jeoljason.com\/wp-content\/uploads\/2022\/03\/13C19F-spectra-perfluorinated-molecule-expansion-1.png?resize=600%2C317&amp;ssl=1 600w, https:\/\/i0.wp.com\/www.jeoljason.com\/wp-content\/uploads\/2022\/03\/13C19F-spectra-perfluorinated-molecule-expansion-1.png?resize=700%2C370&amp;ssl=1 700w, https:\/\/i0.wp.com\/www.jeoljason.com\/wp-content\/uploads\/2022\/03\/13C19F-spectra-perfluorinated-molecule-expansion-1.png?resize=768%2C406&amp;ssl=1 768w, https:\/\/i0.wp.com\/www.jeoljason.com\/wp-content\/uploads\/2022\/03\/13C19F-spectra-perfluorinated-molecule-expansion-1.png?resize=800%2C423&amp;ssl=1 800w, https:\/\/i0.wp.com\/www.jeoljason.com\/wp-content\/uploads\/2022\/03\/13C19F-spectra-perfluorinated-molecule-expansion-1.png?resize=1536%2C812&amp;ssl=1 1536w, https:\/\/i0.wp.com\/www.jeoljason.com\/wp-content\/uploads\/2022\/03\/13C19F-spectra-perfluorinated-molecule-expansion-1.png?w=1858&amp;ssl=1 1858w\" sizes=\"(max-width: 898px) 100vw, 898px\" \/><\/p>\n<p>(2) C-5(150.429ppm)\u306e\u5404<sup>19<\/sup>F\u9078\u629e\u7684\u30c7\u30ab\u30c3\u30d7\u30ea\u30f3\u30b0\u30b9\u30da\u30af\u30c8\u30eb<\/p>\n<p>&nbsp;<\/p>\n<p><img data-recalc-dims=\"1\" decoding=\"async\" class=\"alignnone wp-image-1420\" src=\"https:\/\/i0.wp.com\/www.jeoljason.com\/wp-content\/uploads\/2022\/03\/13C19F-spectra-perfluorinated-molecule-expansion-2.png?resize=901%2C472&#038;ssl=1\" alt=\"\" width=\"901\" height=\"472\" srcset=\"https:\/\/i0.wp.com\/www.jeoljason.com\/wp-content\/uploads\/2022\/03\/13C19F-spectra-perfluorinated-molecule-expansion-2.png?resize=200%2C105&amp;ssl=1 200w, https:\/\/i0.wp.com\/www.jeoljason.com\/wp-content\/uploads\/2022\/03\/13C19F-spectra-perfluorinated-molecule-expansion-2.png?resize=300%2C157&amp;ssl=1 300w, https:\/\/i0.wp.com\/www.jeoljason.com\/wp-content\/uploads\/2022\/03\/13C19F-spectra-perfluorinated-molecule-expansion-2.png?resize=400%2C210&amp;ssl=1 400w, https:\/\/i0.wp.com\/www.jeoljason.com\/wp-content\/uploads\/2022\/03\/13C19F-spectra-perfluorinated-molecule-expansion-2.png?resize=500%2C262&amp;ssl=1 500w, https:\/\/i0.wp.com\/www.jeoljason.com\/wp-content\/uploads\/2022\/03\/13C19F-spectra-perfluorinated-molecule-expansion-2.png?resize=600%2C315&amp;ssl=1 600w, https:\/\/i0.wp.com\/www.jeoljason.com\/wp-content\/uploads\/2022\/03\/13C19F-spectra-perfluorinated-molecule-expansion-2.png?resize=700%2C367&amp;ssl=1 700w, https:\/\/i0.wp.com\/www.jeoljason.com\/wp-content\/uploads\/2022\/03\/13C19F-spectra-perfluorinated-molecule-expansion-2.png?resize=768%2C403&amp;ssl=1 768w, https:\/\/i0.wp.com\/www.jeoljason.com\/wp-content\/uploads\/2022\/03\/13C19F-spectra-perfluorinated-molecule-expansion-2.png?resize=800%2C419&amp;ssl=1 800w, https:\/\/i0.wp.com\/www.jeoljason.com\/wp-content\/uploads\/2022\/03\/13C19F-spectra-perfluorinated-molecule-expansion-2.png?resize=1024%2C537&amp;ssl=1 1024w, https:\/\/i0.wp.com\/www.jeoljason.com\/wp-content\/uploads\/2022\/03\/13C19F-spectra-perfluorinated-molecule-expansion-2.png?resize=1200%2C629&amp;ssl=1 1200w, https:\/\/i0.wp.com\/www.jeoljason.com\/wp-content\/uploads\/2022\/03\/13C19F-spectra-perfluorinated-molecule-expansion-2.png?resize=1536%2C805&amp;ssl=1 1536w, https:\/\/i0.wp.com\/www.jeoljason.com\/wp-content\/uploads\/2022\/03\/13C19F-spectra-perfluorinated-molecule-expansion-2.png?w=1810&amp;ssl=1 1810w\" sizes=\"(max-width: 901px) 100vw, 901px\" \/><\/p>\n<p>(3) \u56db\u7d1a\u70ad\u7d20C-4(90.881ppm)\u306e\u5404<sup>19<\/sup>F\u9078\u629e\u7684\u30c7\u30ab\u30c3\u30d7\u30ea\u30f3\u30b0\u30b9\u30da\u30af\u30c8\u30eb<\/p>\n<p>&nbsp;<\/p>\n<p>\u6700\u5f8c\u306b\u3001<sup>19<\/sup>F-<sup>13<\/sup>C\u30ab\u30c3\u30d7\u30ea\u30f3\u30b0\u3068\u4f8b\u306b\u6319\u3052\u305f\u5206\u5b50\u3059\u3079\u3066\u306e\u5e30\u5c5e\u3092\u8a18\u3057\u305f\u8868\u3092\u793a\u3057\u307e\u3059\u3002<\/p>\n<p><img data-recalc-dims=\"1\" 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JASON\u30bd\u30d5\u30c8\u30a6\u30a7\u30a2<\/a>\u3092\u8a66\u3057\u3066\u307f\u3066\u3001\u76f4\u611f\u7684\u306a\u30e6\u30fc\u30b6\u30fc\u30a4\u30f3\u30bf\u30fc\u30d5\u30a7\u30fc\u30b9\u3084\u9ad8\u5ea6\u306a\u30c7\u30fc\u30bf\u51e6\u7406\u3001\u89e3\u6790\u30c4\u30fc\u30eb\u304c\u3042\u306a\u305f\u306e\u751f\u7523\u6027\u3092\u9ad8\u3081\u308b\u65b9\u6cd5\u3092\u767a\u898b\u3057\u3066\u307f\u307e\u305b\u3093\u304b\u3002\u3082\u3057\u65b0\u4e16\u4ee3<u>\u5206\u5149\u8a08<\/u>\u3084<u>\u30d7\u30ed\u30fc\u30d6<\/u>\u306b\u3064\u3044\u3066\u3082\u3063\u3068\u77e5\u308a\u305f\u3044\u5834\u5408\u306f\u30ea\u30f3\u30af\u5148\u3092\u30af\u30ea\u30c3\u30af\u3057\u3066\u304f\u3060\u3055\u3044\u3002<\/p>\n<p>&nbsp;<\/p>\n<p>&nbsp;<\/p>\n","protected":false},"excerpt":{"rendered":"<p>NMR\u5206\u5149\u6cd5\u306b\u304a\u3044\u3066  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